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Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.
Nákup knihy
X-Ray Structure Determination, George H. Stout
- Jazyk
- Rok vydania
- 1989
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- Titul
- X-Ray Structure Determination
- Podtitul
- A Practical Guide, 2nd Edition
- Jazyk
- anglicky
- Autori
- George H. Stout
- Vydavateľ
- Wiley-Interscience
- Rok vydania
- 1989
- Väzba
- pevná
- Počet strán
- 480
- ISBN10
- 0471607118
- ISBN13
- 9780471607113
- Série
- Štítky
- Veda, Technológia, Fyzika, Chémia, Vedecké teórie, Fyzikálna chémia, Krystalografia
- Anotácia
- Closely follows an actual structural determination. After some introductory material on the nature of x-rays, the diffraction process, and the internal geometry of crystals, the selection and preparation of a crystal are considered. Techniques of measuring raw x-ray data are covered, plus their reduction into a useable form. The second part discusses both traditional and novel methods of solving the ``phase'' problem, the principal difficulty in x-ray structure determination. The third part considers how to extract the most information from the data and how to evaluate its reliability. Finally, there is a discussion of sources of error in practice and interpretation.